REPORTING LIMITS

SEMIVOLATILE ORGANICS

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Extractable Hydrocarbons (TPH-D) EPA 8015B

CAS # Compound Water RL ug/L Soil RL mg/Kg 68334-30-5 Diesel 50 1 Additional Compounds (may be added to the compound list): Bunker C 300 5 Commercial Jet Fuel 50 1 JP-5 Jet Fuel 50 1 Kerosene 50 1 Hydraulic Fluid 300 5 Motor Oil 300 5 Transformer Oil 300 5 Surrogates 630-01-3 Hexacosane

Chlorinated Pesticides EPA 8081A

CAS # Compound Water RL ug/L Soil RL ug/Kg 309-00-2 Aldrin 0.05 1.7 319-84-6 alpha-BHC 0.05 1.7 319-85-7 beta-BHC 0.05 1.7 319-86-8 delta-BHC 0.05 1.7 58-89-9 gamma-BHC (Lindane) 0.05 1.7 5103-71-9 alpha-Chlordane 0.05 1.7 5103-74-2 gamma-Chlordane 0.05 1.7 72-54-8 4,4'-DDD 0.1 3.3 72-55-9 4,4'-DDE 0.1 3.3 50-29-3 4,4'-DDT 0.1 3.3 60-57-1 Dieldrin 0.1 3.3 959-98-8 Endosulfan I 0.05 1.7 33213-65-9 Endosulfan II 0.1 3.3 1031-07-8 Endosulfan sulfate 0.1 3.3 72-20-8 Endrin 0.1 3.3 7421-93-4 Endrin aldehyde 0.1 3.3 76-44-8 Heptachlor 0.05 1.7 1024-57-3 Heptachlor epoxide A 0.05 1.7 1024-57-3 Heptachlor epoxide B 0.05 1.7 72-43-5 Methoxychlor 0.5 17 8001-35-2 Toxaphene 1 60 Additional Compounds (may be added to the compound list): 57-74-9 Chlordane (technical) 0.5 30 53494-70-5 Endrin ketone 0.1 3.3 Surrogates: 2051-24-3 Decachlorobiphenyl (DCB) 877-35-2 Tetrachloro-m-xylene (TCMX)

Polychlorinated Biphenyls (PCB) EPA 8082

CAS # Compound Water RL ug/L Soil RL ug/Kg 12674-11-2 Aroclor-1016 0.5 12 11104-28-2 Aroclor-1221 1 24 11141-16-5 Aroclor-1232 0.5 12 53469-21-9 Aroclor-1242 0.5 12 12672-29-6 Aroclor-1248 0.5 12 11097-69-1 Aroclor-1254 0.5 12 11096-82-5 Aroclor-1260 0.5 12 Surrogates: 2051-24-3 Decachlorobiphenyl (DCB) 877-35-2 Tetrachloro-m-xylene (TCMX)

Semivolatile Organics EPA 8270C

CAS # Compound Water RL ug/L Soil RL ug/Kg 83-32-9 Acenaphthene 10 67 208-96-8 Acenaphthylene 10 67 120-12-7 Anthracene 10 67 103-33-3 Azobenzene 10 330 56-55-3 Benzo(a)anthracene 10 67 50-32-8 Benzo(a)pyrene 10 67 205-99-2 Benzo(b)fluoranthene 10 67 207-08-9 Benzo(k)fluoranthene 10 67 191-24-2 Benzo(g,h,i)perylene 10 67 65-85-0 Benzoic acid 50 1,700 100-51-6 Benzyl alcohol 10 330 111-91-1 bis(2-Chloroethoxy)methane 10 330 111-44-4 bis(2-Chloroethyl)ether 10 330 108-60-1 bis(2-Chloroisopropyl)ether 10 330 117-81-7 bis(2-Ethylhexyl)phthalate 10 330 101-55-3 4-Bromophenyl-phenylether 10 330 85-68-7 Butylbenzylphthalate 10 330 106-47-8 4-Chloroaniline 10 330 59-50-7 4-Chloro-3-methylphenol 10 330 91-58-7 2-Chloronaphthalene 10 330 95-57-8 2-Chlorophenol 10 330 7005-72-3 4-Chlorophenyl-phenylether 10 330 218-01-9 Chrysene 10 67 53-70-3 Dibenz(a,h)anthracene 10 67 132-64-9 Dibenzofuran 10 330 95-50-1 1,2-Dichlorobenzene 10 330 541-73-1 1,3-Dichlorobenzene 10 330 106-46-7 1,4-Dichlorobenzene 10 330 91-94-1 3,3'-Dichlorobenzidine 20 670 120-83-2 2,4-Dichlorophenol 10 330 84-66-2 Diethylphthalate 10 330 105-67-9 2,4-Dimethylphenol 10 330 131-11-3 Dimethylphthalate 10 330 84-74-2 Di-n-butylphthalate 10 330 534-52-1 4,6-Dinitro-2-methylphenol 20 670 51-28-5 2,4-Dinitrophenol 20 670 121-14-2 2,4-Dinitrotoluene 10 330 606-20-2 2,6-Dinitrotoluene 10 330 117-84-0 Di-n-octylphthalate 10 330 206-44-0 Fluoranthene 10 67 86-73-7 Fluorene 10 67 118-74-1 Hexachlorobenzene 10 330 87-68-3 Hexachlorobutadiene 10 330 77-47-4 Hexachlorocyclopentadiene 20 670 67-72-1 Hexachloroethane 10 330 193-39-5 Indeno(1,2,3-cd)pyrene 10 67 78-59-1 Isophorone 10 330 91-57-6 2-Methylnaphthalene 10 67 95-48-7 2-Methylphenol 10 330 1319-77-3 4-Methylphenol (coelutes w/ 3-) 10 330 88-74-4 2-Nitroaniline 20 670 99-09-2 3-Nitroaniline 20 670 100-01-6 4-Nitroaniline 20 670 88-75-5 2-Nitrophenol 20 670 100-02-7 4-Nitrophenol 20 670 621-64-7 N-Nitroso-di-n-propylamine 10 330 62-75-9 N-Nitrosodimethylamine 10 330 86-30-6 N-Nitrosodiphenylamine 10 330 91-20-3 Naphthalene 10 67 98-95-3 Nitrobenzene 10 330 87-86-5 Pentachlorophenol 20 670 85-01-8 Phenanthrene 10 67 108-95-2 Phenol 10 330 129-00-0 Pyrene 10 67 120-82-1 1,2,4-Trichlorobenzene 10 330 95-95-4 2,4,5-Trichlorophenol 10 330 88-06-2 2,4,6-Trichlorophenol 10 330 Additional Compounds (may be added to the compound list): 62-53-3 Aniline 10 330 92-87-5 Benzidine 10 330 110-86-1 Pyridine 100 1,700 Surrogates: 321-60-8 2-Fluorobiphenyl 367-12-4 2-Fluorophenol 4165-60-0 Nitrobenzene-d5 13127-88-3 Phenol-d5 1718-51-0 Terphenyl-d14 118-79-6 2,4,6-Tribromophenol

Phenolic Compounds EPA 8270C

CAS # Compound Water RL ug/L Soil RL ug/Kg 59-50-7 4-Chloro-3-methylphenol 10 330 95-57-8 2-Chlorophenol 10 330 120-83-2 2,4-Dichlorophenol 10 330 105-67-9 2,4-Dimethylphenol 10 330 534-52-1 4,6-Dinitro-2-methylphenol 20 670 51-28-5 2,4-Dinitrophenol 20 670 95-48-7 2-Methylphenol 10 330 1319-77-3 4-Methylphenol (coelutes w/ 3-) 10 330 88-75-5 2-Nitrophenol 20 670 100-02-7 4-Nitrophenol 20 670 87-86-5 Pentachlorophenol 20 670 108-95-2 Phenol 10 330 95-95-4 2,4,5-Trichlorophenol 10 330 88-06-2 2,4,6-Trichlorophenol 10 330 Surrogates: 367-12-4 2-Fluorophenol 13127-88-3 Phenol-d5 118-79-6 2,4,6-Tribromophenol

Phthalates EPA 8270C

CAS # Compound Water RL ug/L Soil RL ug/Kg 117-81-7 bis(2-Ethylhexyl)phthalate 10 330 85-68-7 Butylbenzylphthalate 10 330 84-66-2 Diethylphthalate 10 330 131-11-3 Dimethylphthalate 10 330 84-74-2 Di-n-butylphthalate 10 330 117-84-0 Di-n-octylphthalate 10 330 Surrogates: 321-60-8 2-Fluorobiphenyl 4165-60-0 Nitrobenzene-d5 1718-51-0 Terphenyl-d14

Polynuclear Aromatic Hydrocarbons (PAH) EPA 8270

CAS # Compound Water RL ug/L Soil RL ug/Kg 83-32-9 Acenaphthene 10 67 208-96-8 Acenaphthylene 10 67 120-12-7 Anthracene 10 67 56-55-3 Benzo(a)anthracene 10 67 50-32-8 Benzo(a)pyrene 10 67 205-99-2 Benzo(b)fluoranthene 10 67 207-08-9 Benzo(k)fluoranthene 10 67 191-24-2 Benzo(g,h,i)perylene 10 67 218-01-9 Chrysene 10 67 53-70-3 Dibenz(a,h)anthracene 10 67 206-44-0 Fluoranthene 10 67 86-73-7 Fluorene 10 67 193-39-5 Indeno(1,2,3-cd)pyrene 10 67 91-20-3 Naphthalene 10 67 85-01-8 Phenanthrene 10 67 129-00-0 Pyrene 10 67 Surrogates: 321-60-8 2-Fluorobiphenyl 4165-60-0 Nitrobenzene-d5 1718-51-0 Terphenyl-d14

Polynuclear Aromatic Hydrocarbons (PAH) EPA 8270-SIM

CAS # Compound Water RL ug/L Soil RL ug/Kg 83-32-9 Acenaphthene 0.1 5 208-96-8 Acenaphthylene 0.1 5 120-12-7 Anthracene 0.1 5 56-55-3 Benzo(a)anthracene 0.1 5 50-32-8 Benzo(a)pyrene 0.1 5 205-99-2 Benzo(b)fluoranthene 0.1 5 207-08-9 Benzo(k)fluoranthene 0.1 5 191-24-2 Benzo(g,h,i)perylene 0.1 5 218-01-9 Chrysene 0.1 5 53-70-3 Dibenz(a,h)anthracene 0.1 5 206-44-0 Fluoranthene 0.1 5 86-73-7 Fluorene 0.1 5 193-39-5 Indeno(1,2,3-cd)pyrene 0.1 5 91-20-3 Naphthalene 0.1 5 85-01-8 Phenanthrene 0.1 5 129-00-0 Pyrene 0.1 5 Surrogates: 321-60-8 2-Fluorobiphenyl 4165-60-0 Nitrobenzene-d5 1718-51-0 Terphenyl-d14

Polynuclear Aromatic Hydrocarbons (PAH) EPA 8310

CAS # Compound Water RL ug/L Soil RL ug/Kg 83-32-9 Acenaphthene 1 33 208-96-8 Acenaphthylene 2 67 120-12-7 Anthracene 0.1 3.3 56-55-3 Benzo(a)anthracene 0.1 3.3 50-32-8 Benzo(a)pyrene 0.1 3.3 205-99-2 Benzo(b)fluoranthene 0.2 6.7 191-24-2 Benzo(g,h,i)perylene 0.2 6.7 207-08-9 Benzo(k)fluoranthene 0.1 3.3 218-01-9 Chrysene 0.1 3.3 53-70-3 Dibenz(a,h)anthracene 0.2 6.7 206-44-0 Fluoranthene 0.2 6.7 86-73-7 Fluorene 0.2 6.7 193-39-5 Indeno(1,2,3-cd)pyrene 0.1 3.3 91-20-3 Naphthalene 1 33 85-01-8 Phenanthrene 0.1 3.3 129-00-0 Pyrene 0.1 3.3 Surrogates: 90-12-0 1-Methylnaphthalene

Nitroaromatics & Nitramines (Explosives) EPA 8330

CAS # Compound Water RL ug/L Soil RL ug/Kg 2691-41-0 HMX 1 200 121-82-4 RDX 1 200 99-35-4 1,3,5-Trinitrobenzene 1 200 99-65-0 1,3-Dinitrobenzene 1 200 98-95-3 Nitrobenzene 1 200 479-45-8 Tetryl 1 200 118-96-7 2,4,6-Trinitrotoluene 1 200 35572-78-2 2-Amino-4,6-dinitrotoluene 1 200 1946-51-0 4-Amino-2,6-dinitrotoluene 1 200 121-14-2 2,4-Dinitrotoluene 1 200 606-20-2 2,6-Dinitrotoluene 1 200 88-72-2 2-Nitrotoluene 1 400 99-99-0 4-Nitrotoluene 1 400 99-08-1 3-Nitrotoluene 1 400 Surrogate: 90-12-0 1-Methylnaphthalene